2D In‐Plane Molecular Superlattice Heterojunctions for High‐Performance Ambipolar Electronics and Low‐Dose X‐Ray Sensing

M Miaoyu Wang (The International Joint Institute of Tianjin University Tianjin University Fuzhou China) S Shuyu Li (State Key Laboratory for Crop Stress Resistance and High-Efficiency Production, Shaanxi Key Laboratory of Agricultural and Environmental Microbiology, College of Life Sciences, Northwest Agriculture and Forestry University) L Lingjie Sun (State Key Laboratory of Advanced Materials for Intelligent Sensing, Key Laboratory of Organic Integrated Circuit, Ministry of Education & Tianjin Key Laboratory of Molecular Optoelectronic Sciences, Department of Chemistry, School of Science & Institute of Molecular Aggregation Science, Tianjin University) Y Yiwen Ren (State Key Laboratory of Advanced Materials for Intelligent Sensing Key Laboratory of Organic Integrated Circuit Ministry of Education & Tianjin Key Laboratory of Molecular Optoelectronic Sciences Department of Chemistry Institute of Molecular Aggregation Science & School of Science Tianjin University Tianjin China) X Xianshuo Wu (Key Laboratory of Organic Integrated Circuit, Ministry of Education & Tianjin Key Laboratory of Molecular Optoelectronic Sciences, Department of Chemistry, School of Science, Tianjin University) J Jiayuan Wang W Wenbin Shi Z Zongbo Feng (State Key Laboratory of Advanced Materials for Intelligent Sensing Key Laboratory of Organic Integrated Circuit Ministry of Education & Tianjin Key Laboratory of Molecular Optoelectronic Sciences Department of Chemistry Institute of Molecular Aggregation Science & School of Science Tianjin University Tianjin China) S Shuaishuai Ding (State Key Laboratory of Advanced Materials for Intelligent Sensing, Key Laboratory of Organic Integrated Circuit, Ministry of Education & Tianjin Key Laboratory of Molecular Optoelectronic Sciences, Department of Chemistry, Institute of Molecular Aggregation Science, School of Science) R Ran Ding (State Key Laboratory of Integrated Optoelectronics, College of Electronic Science and Engineering) F Fangxu Yang (Key Laboratory of Organic Integrated Circuit, Ministry of Education & Tianjin Key Laboratory of Molecular Optoelectronic Sciences, Department of Chemistry, School of Science, Tianjin University) X Xiaotao Zhang (Tianjin Key Laboratory of Molecular Optoelectronic Sciences, Department of Chemistry, School of Science, Tianjin University and Collaborative Innovation Center of Chemical Science and Engineering, Tianjin 300072, China) W Wenping Hu

Abstract

ABSTRACT Two‐dimensional in‐plane molecular superlattice heterojunctions, where distinct semiconducting components are integrated laterally within a single crystalline plane, offer an ideal architecture for controlling charge separation and transport in optoelectronic devices. However, realizing such structures with molecular‐level precision, long‐range periodicity, and sharp interfaces in organic semiconductors remains a major challenge. Here, the first 2D organic heterojunction featuring long‐range, in‐plane donor–acceptor superlattice via cocrystal engineering is presented. By employing phase‐separated molecular design for the donor (TIPS‐PEN) and acceptor (PDI‐FCN), strong in‐plane cohesion is decoupled from out‐of‐plane steric repulsion, inducing a periodic –D–A–D– arrangement within the crystal plane. The resulting high‐density, lattice‐defined heterointerfaces facilitate exciton dissociation, directional charge transport, and efficient extraction. The ultrathin crystal enables effective gate‐field control, yielding ambipolar OFETs with exceptional on/off ratios of 10 8 (holes) and 10 7 (electrons). Capitalizing on the narrow bandgap and the ordered 2D heterointerface, this material demonstrates outstanding high‐energy photon conversion efficiency. As an X‐ray detector, it exhibits high sensitivity of 4.21 × 10 4 µC Gy −1 cm −2 and low detection limit 5.73 nGy s −1 , enabling clear imaging at 14.77 nGy s −1 ultralow dose rate. This work provides new ideas for constructing 2D multicomponent organic heterostructures and unlocks potential for next‐generation flexible electronics and low‐dose radiation sensing.

Article Details

Volume / Issue Vol. 38, Issue 46
Published August 01, 2026
ISSN 0935-9648
Publisher Unknown Publisher

Journal Info

Advanced Materials

Unknown Publisher

ISSN: 0935-9648 Physical Sciences

Authors (13)

M

Miaoyu Wang

The International Joint Institute of Tianjin University Tianjin University Fuzhou China

S

Shuyu Li

State Key Laboratory for Crop Stress Resistance and High-Efficiency Production, Shaanxi Key Laboratory of Agricultural and Environmental Microbiology, College of Life Sciences, Northwest Agriculture and Forestry University

L

Lingjie Sun

State Key Laboratory of Advanced Materials for Intelligent Sensing, Key Laboratory of Organic Integrated Circuit, Ministry of Education & Tianjin Key Laboratory of Molecular Optoelectronic Sciences, Department of Chemistry, School of Science & Institute of Molecular Aggregation Science, Tianjin University

Y

Yiwen Ren

State Key Laboratory of Advanced Materials for Intelligent Sensing Key Laboratory of Organic Integrated Circuit Ministry of Education & Tianjin Key Laboratory of Molecular Optoelectronic Sciences Department of Chemistry Institute of Molecular Aggregation Science & School of Science Tianjin University Tianjin China

X

Xianshuo Wu

Key Laboratory of Organic Integrated Circuit, Ministry of Education & Tianjin Key Laboratory of Molecular Optoelectronic Sciences, Department of Chemistry, School of Science, Tianjin University

J

Jiayuan Wang

W

Wenbin Shi

Z

Zongbo Feng

State Key Laboratory of Advanced Materials for Intelligent Sensing Key Laboratory of Organic Integrated Circuit Ministry of Education & Tianjin Key Laboratory of Molecular Optoelectronic Sciences Department of Chemistry Institute of Molecular Aggregation Science & School of Science Tianjin University Tianjin China

S

Shuaishuai Ding

State Key Laboratory of Advanced Materials for Intelligent Sensing, Key Laboratory of Organic Integrated Circuit, Ministry of Education & Tianjin Key Laboratory of Molecular Optoelectronic Sciences, Department of Chemistry, Institute of Molecular Aggregation Science, School of Science

R

Ran Ding

State Key Laboratory of Integrated Optoelectronics, College of Electronic Science and Engineering

F

Fangxu Yang

Key Laboratory of Organic Integrated Circuit, Ministry of Education & Tianjin Key Laboratory of Molecular Optoelectronic Sciences, Department of Chemistry, School of Science, Tianjin University

X

Xiaotao Zhang

Tianjin Key Laboratory of Molecular Optoelectronic Sciences, Department of Chemistry, School of Science, Tianjin University and Collaborative Innovation Center of Chemical Science and Engineering, Tianjin 300072, China

W

Wenping Hu