Stabilizing Sputtered NiO <sub>x</sub> via In Situ Dissociative Adsorption Passivation for Efficient Perovskite Solar Cells

C Chenghao Ge H Huanyu Zhang S Shikai Chang (State Key Laboratory of Bioinspired Interfacial Materials Science Institute of Functional Nano &amp; Soft Materials (FUNSOM) Soochow University Suzhou China) K Kaixin Du (State Key Laboratory of Bioinspired Interfacial Materials Science Institute of Functional Nano &amp; Soft Materials (FUNSOM) Soochow University Suzhou China) Y Yang Li Y Yi Ji (State Key Laboratory of Catalysis) S Shuilong Kang (State Key Laboratory of Bioinspired Interfacial Materials Science, Institute of Functional Nano & Soft Materials (FUNSOM)) R Rongbin Wang Y Yanbo Wang (Department of Materials Science and Engineering, City University of Hong Kong) Y Yansen Guo (State Key Laboratory of Bioinspired Interfacial Materials Science Institute of Functional Nano &amp; Soft Materials (FUNSOM) Soochow University Suzhou China) Z Zewu Feng (State Key Laboratory of Bioinspired Interfacial Materials Science Institute of Functional Nano &amp; Soft Materials (FUNSOM) Soochow University Suzhou China) X Xueqi Wu Y Yitong Liu (Peking-Tsinghua Center for Life Science, Academy for Advanced Interdisciplinary Studies, Peking University) X Xin Li Y Yige Peng (State Key Laboratory of Bioinspired Interfacial Materials Science Institute of Functional Nano &amp; Soft Materials (FUNSOM) Soochow University Suzhou China) Y Yinhua Li (State Key Laboratory of Bioinspired Interfacial Materials Science Institute of Functional Nano &amp; Soft Materials (FUNSOM) Soochow University Suzhou China) Y Yunhao Liang (State Key Laboratory of Bioinspired Interfacial Materials Science Institute of Functional Nano &amp; Soft Materials (FUNSOM) Soochow University Suzhou China) Y Yang Zhang S Shipeng Yu (State Key Laboratory of Bioinspired Interfacial Materials Science Institute of Functional Nano &amp; Soft Materials (FUNSOM) Soochow University Suzhou China) Y Yurou Zhang (Beijing National Laboratory for Molecular Sciences, College of Chemistry and Molecular Engineering) C Chaopeng Huang (Zhejiang Baima Lake Laboratory Co., Ltd. Hangzhou China) N Na Li J Jingsong Sun (Zhejiang Baima Lake Laboratory Co., Ltd. Hangzhou China) Z Zhongyao Jiang (Laoshan Laboratory) H Haifeng Gao X Xuran Zhu (China Electric Power Research Institute Co., Ltd. Beijing China) Y Youyong Li (Institute of Functional Nano & Soft Materials (FUNSOM), Jiangsu Key Laboratory for Carbon-Based Functional Materials & Devices) X Xiao‐Hong Zhang (Institute of Functional Nano &amp; Soft Materials (FUNSOM) Joint International Research Laboratory of Carbon‐Based Functional Materials and Devices Soochow University Suzhou Jiangsu P. R. China) J Jun Peng (State Key Laboratory of Physical Chemistry of Solid Surfaces, Department of Chemistry)

Abstract

ABSTRACT Sputtered nickel oxide (NiO x ) is an industrially compatible hole transport layer for perovskite solar cells (PSCs), yet its practical deployment is limited by interfacial instability arising from disordered Ni 3+ species and unfavorable reactions with perovskite absorbers. Here, we introduce an in situ dissociative adsorption passivation (IDAP) strategy using bromoacetamide (BAA) to stabilize sputtered NiO x . In this approach, Br − ions act as site‐blockers by coordinating with surface Ni, suppressing interfacial disorder and stabilizing Ni 3+ species, while the amide group provides dual anchoring: N−H···O hydrogen bonding strengthens attachment to NiO x , and the carbonyl group (C═O) passivates the uncoordinated Pb 2+ located at or near the interface between the NiO x and the perovskite films. These cooperative efforts reduce trap states, suppress interfacial redox reactions, and mitigate defect‐driven degradation under thermal stress. PSCs incorporating BAA‐NiO x achieve a champion power conversion efficiency (PCE) of 26.31% along with a certified PCE of 26.07%, while the larger‐area PSCs (1 cm 2 ) maintain 25.48% efficiency. This is one of the highest efficiencies reported for NiO x ‐based PSCs. In addition, the encapsulated cell retains 93% of its initial performance after 1500 h of continuous operation.

Article Details

Volume / Issue Vol. 38, Issue 34
Published June 01, 2026
ISSN 0935-9648
Publisher Unknown Publisher

Journal Info

Advanced Materials

Unknown Publisher

ISSN: 0935-9648 Physical Sciences

Authors (29)

C

Chenghao Ge

H

Huanyu Zhang

S

Shikai Chang

State Key Laboratory of Bioinspired Interfacial Materials Science Institute of Functional Nano &amp; Soft Materials (FUNSOM) Soochow University Suzhou China

K

Kaixin Du

State Key Laboratory of Bioinspired Interfacial Materials Science Institute of Functional Nano &amp; Soft Materials (FUNSOM) Soochow University Suzhou China

Y

Yang Li

Y

Yi Ji

State Key Laboratory of Catalysis

S

Shuilong Kang

State Key Laboratory of Bioinspired Interfacial Materials Science, Institute of Functional Nano & Soft Materials (FUNSOM)

R

Rongbin Wang

Y

Yanbo Wang

Department of Materials Science and Engineering, City University of Hong Kong

Y

Yansen Guo

State Key Laboratory of Bioinspired Interfacial Materials Science Institute of Functional Nano &amp; Soft Materials (FUNSOM) Soochow University Suzhou China

Z

Zewu Feng

State Key Laboratory of Bioinspired Interfacial Materials Science Institute of Functional Nano &amp; Soft Materials (FUNSOM) Soochow University Suzhou China

X

Xueqi Wu

Y

Yitong Liu

Peking-Tsinghua Center for Life Science, Academy for Advanced Interdisciplinary Studies, Peking University

X

Xin Li

Y

Yige Peng

State Key Laboratory of Bioinspired Interfacial Materials Science Institute of Functional Nano &amp; Soft Materials (FUNSOM) Soochow University Suzhou China

Y

Yinhua Li

State Key Laboratory of Bioinspired Interfacial Materials Science Institute of Functional Nano &amp; Soft Materials (FUNSOM) Soochow University Suzhou China

Y

Yunhao Liang

State Key Laboratory of Bioinspired Interfacial Materials Science Institute of Functional Nano &amp; Soft Materials (FUNSOM) Soochow University Suzhou China

Y

Yang Zhang

S

Shipeng Yu

State Key Laboratory of Bioinspired Interfacial Materials Science Institute of Functional Nano &amp; Soft Materials (FUNSOM) Soochow University Suzhou China

Y

Yurou Zhang

Beijing National Laboratory for Molecular Sciences, College of Chemistry and Molecular Engineering

C

Chaopeng Huang

Zhejiang Baima Lake Laboratory Co., Ltd. Hangzhou China

N

Na Li

J

Jingsong Sun

Zhejiang Baima Lake Laboratory Co., Ltd. Hangzhou China

Z

Zhongyao Jiang

Laoshan Laboratory

H

Haifeng Gao

X

Xuran Zhu

China Electric Power Research Institute Co., Ltd. Beijing China

Y

Youyong Li

Institute of Functional Nano & Soft Materials (FUNSOM), Jiangsu Key Laboratory for Carbon-Based Functional Materials & Devices

X

Xiao‐Hong Zhang

Institute of Functional Nano &amp; Soft Materials (FUNSOM) Joint International Research Laboratory of Carbon‐Based Functional Materials and Devices Soochow University Suzhou Jiangsu P. R. China

J

Jun Peng

State Key Laboratory of Physical Chemistry of Solid Surfaces, Department of Chemistry